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Z221171

Sigma-Aldrich

Aldrich® sublimation apparatus

capacity, ≤ 3 g starting material

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1 EA
653,00 €

653,00 €

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1 EA
653,00 €

About This Item

Code UNSPSC :
41121800
Nomenclature NACRES :
NB.43

653,00 €

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Caractéristiques

capacity≤ 3 g starting material

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Catégories apparentées

Description générale

With reversed, screw-thread ST joint and 2 mm glass stopcock. O-ring seals joint without grease, thus eliminating contamination when removing sublimator head. Flat-bottom on inner tube for easy sample removal.

Operation:
1. Place material to be sublimated in bottom of lower vessel
2. Attach condenser assembly to the lower vessel and tighten red cap nut
3. Connect coolant supply hose to upper hose connector and coolant return hose to lower connector
4. Connect vacuum source to stopcock hose connection
5. Place lower vessel into heating mantle, sand bath or high temperature silicone oil bath
6. Use a laboratory thermometer or thermocouple in the mantle, sand or oil to monitor temperature
7. Start flow of coolant through condenser assembly
8. Evacuate lower vessel
9. Turn on heating mantle
10. Sublimation begins

Components:
Z557072, Aldrich sublimation head, for Z221163
Z557056, Aldrich sublimation head, for Z221171
Z557080, Aldrich sublimation reservoir, for Z221163
Z557064, Aldrich sublimation reservoir, for Z221171

Informations légales

Aldrich is a registered trademark of Sigma-Aldrich Co. LLC

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Certificats d'analyse (COA)

Lot/Batch Number

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Questions

1–2 of 2 Questions  

  1. What is the Department of Transportation shipping information for this product?

    1 answer

    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

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  2. Are the hose barbs for Product Z231215 the same as those on Product Z221171? And what is the approximate outside diameter? And what type of tubing should I use?

    1 answer

    1. All three dimensions (as shown by the red arrows in the image below) are the same:The hose barbs for Product Z231215 are the same as those on the Z221171 (approximately 5/16 inch outside diameter).Heavy-walled tubing with an inside diameter of 1/4 in (approx. 6 mm) would work fine. The outside diameter of the hose barb is around 5/16 in (8 mm). You want the tubing to stretch a little bit so that you get a tight seal.

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