- Synthesis of the beta-D-glucuronides of 2,3-, 3,4-, and 2,6-dichlorophenol.
Synthesis of the beta-D-glucuronides of 2,3-, 3,4-, and 2,6-dichlorophenol.
Archiv der Pharmazie (2001-04-24)
S Goenechea, G Rücker, M A Hubert
PMID11315335
ABSTRACT
The beta-D-glucuronides of 2,3-, 3,4-, and 2,6-dichlorophenol (1-3) were prepared by a modified Koenigs-Knorr synthesis. As the alkaline hydrolysis of perpivaloylated methyl (2,3-dichlorophenyl)-glucuronate 1a led to a dehydrated glucuronide, the preparation of peracetylated methyl dichlorophenylglucuronates with subsequent cleavage of the ester bindings under mild conditions was preferred.
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