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[Studies on the chemical constituents of Laportea bulbifera].

Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials (2011-08-10)
Zhu Zhu, Lin Ma, Hai-yan Zhu, Xiao-sheng Yang, Xiao-jiang Hao
ABSTRACT

To study the chemical constituents of Laportea bulbifera. 70% EtOH was used for constituent extraction, silica gel column chromatography for constituent seperation, physical and chemical properties together with spectroscopic methods for chemical structure identification. six compounds were obtained from root of L. bulbifera. Their chemical structures were elucidated as p3-sitosterol(1) , P-daucosterol (2), 2,2'-oxy-bis(1-phenylethanol (3), 1-(2-phenylcarbonyloxy acetyl) benzene (4) , methyl linoleate(5),1,4-diphenyl-1,4-butanedione(6). All compounds are isolated from L. bulbifera and among compounds 3 and 4 are reported as natural products for the first time.

MATERIALS
Product Number
Brand
Product Description

Supelco
trans-9,12-Octadecadienoic acid methyl ester, certified reference material, 10 mg/mL in heptane
Sigma-Aldrich
Methyl linolelaidate
Sigma-Aldrich
Methyl linoleate, ≥98% (GC)
Supelco
Methyl linolelaidate, analytical standard
Supelco
Methyl linoleate, analytical standard
Supelco
cis-9,cis-12-Octadecadienoic acid methyl ester, certified reference material, 10 mg/mL in heptane