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US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on Equity-1701 (15 m x 0.10 mm I.D., 0.10 μm), Fast GC Analysis

US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on Equity-1701 (15 m x 0.10 mm I.D., 0.10 μm), Fast GC Analysis suitable for GC

Materiales

Analytical column

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SPB®-608

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SPB®-608

L × I.D. 30 m × 0.53 mm, df 0.50

Columna para GC capilar Equity -1701

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Columna para GC capilar Equity -1701

L × I.D. 30 m × 0.25 mm, df 1.00 μm

Columna para GC capilar Equity -1701

L × I.D. 30 m × 0.53 mm, df 0.50 μm

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 1.00 μm

SLB®-5ms Capillary GC Column

L × I.D. 15 m × 0.10 mm, df 0.10 μm

For use with

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Wheaton wide-mouth bottle

amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 ea

Guard column

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Nonpolar Fused Silica Tubing

L × I.D. 5.0 m × 0.10 mm

Nonpolar Fused Silica Tubing

L × I.D. 5.0 m × 0.25 mm

Nonpolar Fused Silica Tubing

L × I.D. 5.0 m × 0.53 mm

Optional

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Polyimide Sealing Resin

pkg of 5 g

Standard

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Chlordane

certified reference material, 1000 μg/mL in isooctane

Pesticides Matrix Spike Mix

in methanol (varied), PESTANAL®, analytical standard

Camphechlor solution

certified reference material, 1000 μg/mL in isooctane

EPA CLP Organochlorine Pesticide MIx

certified reference material, 2000 μg/mL each component in hexane: toluene (1:1), ampule of 1 mL

required but not provided

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"Y" GlasSeal Connector, Borosilicate Glass

pkg of 1 ea

"Y" Glassseal Connectors

pkg of 1 ea

"Y" Glassseal Connectors

pkg of 3 ea

CONDITIONS

column

Equity-1701, 15 m × 0.10 mm I.D., 0.10 μm (28343-U)

oven

100 °C, 25 °C/min to 280 °C

inj. temp.

225 °C

detector

ECD, 300 °C

carrier gas

hydrogen, 40 cm/sec constant

injection

2 μL, splitless (0.75 min)

liner

4 mm I.D., single taper

sample

50 ppb of a 22 component chlorinated pesticide standard in n-hexane

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