Volatiles

column

SPB-624, 60 m × 0.25 mm I.D., 1.4 μm (24256)

oven

35 °C (4 min), 4 °C/min to 200 °C

inj. temp.

250 °C

scan range

m/z 45-300

carrier gas

helium, 33 cm/sec @ 40 °C

injection

70:1 split

sample

5 ng on column of each component