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  • Simultaneous determination of brazilin and protosappanin B in Caesalpinia sappan by ionic-liquid dispersive liquid-phase microextraction method combined with HPLC.

Simultaneous determination of brazilin and protosappanin B in Caesalpinia sappan by ionic-liquid dispersive liquid-phase microextraction method combined with HPLC.

Chemistry Central journal (2017-11-15)
Zhaoyang Xia, Dongdong Li, Qing Li, Yan Zhang, Wenyi Kang
RESUMEN

The conditions of heating, ionic liquid-based ultrasonic-assisted extraction combined with reverse-phase high performance liquid chromatography were optimized to simultaneously isolate and determinate brazilin and protosappanin B in Caesalpinia sappan. Ionic liquids, including [BMIM]Br, [BMIM]BF

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Sigma-Aldrich
1-Hexyl-3-methylimidazolium hexafluorophosphate, ≥97.0% (HPLC)