GC Analysis of FAMEs in Soybean Oil on SLB-IL111

column

SLB-IL111, 30 m x 0.25 mm I.D., 0.20 μm (28927-U)

oven

180 °C

inj. temp.

250 °C

detector

FID, 260 °C

carrier gas

helium, 25 cm/sec

injection

1 μL, 50:1 split

liner

4 mm I.D., split type, cup design

sample

Characterized reference oils, methylated using BF3-methanol

prior to analysis