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28467-U

Supelco

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.10 μm

Synonym(s):

GC column, SPB-5, 5% diphenyl, mass spec

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About This Item

UNSPSC Code:
12000000
eCl@ss:
32119290
NACRES:
SB.54

material

fused silica

Quality Level

Agency

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

reg. compliance

FDA LIB 4423

parameter

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

Beta value

625

df

0.10 μm

technique(s)

GC/MS: suitable
gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

column type

capillary non-polar

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General description

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded and highly crosslinked
  • Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
  • ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Application

  • An improved method for cyanide determination in blood using solid-phase microextraction and gas chromatography/mass spectrometry.: This study presents an enhanced method for determining cyanide levels in blood, employing solid-phase microextraction combined with gas chromatography/mass spectrometry. This technique improves sensitivity and accuracy, essential for toxicological and forensic analysis (Frison et al., 2006).
  • Photochemical production of conjugated linoleic acid from soybean oil.: This research explores the photochemical production of conjugated linoleic acid (CLA) from soybean oil. The study utilized gas chromatography for the analysis of CLA, demonstrating an efficient method for producing this valuable compound with potential health benefits (Gangidi & Proctor, 2004).
  • Development of a solid-phase microextraction GC-NPD procedure for the determination of free volatile amines in wastewater and sewage-polluted waters.: This work describes the development of a GC-NPD procedure using solid-phase microextraction for detecting volatile amines in wastewater. This method offers improved detection limits and specificity, which are critical for environmental monitoring and water quality assessment (Abalos et al., 1999).

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Alessia Arena et al.
Food chemistry, 396, 133721-133721 (2022-07-24)
Phthalic acid esters (PAEs), known as phthalates, have a variety of industrial applications, mainly related to their ability to increase plastic softness,flexibility, and durability. With regard to toxicological aspects, several studies suggest that phthalates would act as endocrine-disrupting chemicals, and
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction
Annie Xu Zeng et al.
Analytica chimica acta, 803, 166-173 (2013-11-13)
Due to their distinct chemical properties, the application of ionic liquid (IL) compounds as gas chromatography (GC) stationary phases offer unique GC separation especially in the analysis of geometric and positional fatty acid methyl ester (FAME) isomers. Elution behaviour of
Lisa Simonsson et al.
Chemphyschem : a European journal of chemical physics and physical chemistry, 11(5), 1011-1017 (2010-03-20)
We investigate the Ca(2+)-triggered fusion of lipid vesicles site-selectively tethered to a DNA-modified supported lipid bilayer array, with the DNA strands designed such that hybridization occurs in a zipperlike fashion. Prior to the addition of Ca(2+), which is observed to
Noelia Aldai et al.
Journal of agricultural and food chemistry, 66(4), 842-855 (2018-01-02)
Incubation of DHA with sheep rumen fluid resulted in 80% disappearance in 6 h. The products were analyzed as their fatty acid (FA) methyl esters by GC-FID on SP-2560 and SLB-IL111 columns. The GC-online reduction × GC and GC-MS techniques

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Sigma-Aldrich presents an article about the analysis of melamine and related compounds in dog food with the use of more economical gas chromatography-mass spectrometry (GC-MS) instrumentation.

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This page is intended to make it easier to find the consumables you need based on the analytical method you’re using. Methods included on this page come from the EPA, Standard Methods and ASTM.

This page is intended to make it easier to find the consumables you need based on the analytical method you’re using. Methods included on this page come from the EPA, Standard Methods and ASTM.

This page is intended to make it easier to find the consumables you need based on the analytical method you’re using. Methods included on this page come from the EPA, Standard Methods and ASTM.

This page is intended to make it easier to find the consumables you need based on the analytical method you’re using. Methods included on this page come from the EPA, Standard Methods and ASTM.

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