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Merck

Acetaldehyde, methanol, and ethanol analysis by headspace gas chromatography.

Journal of analytical toxicology (1980-01-01)
R M Anthony, C A Sutheimer, I Sunshine
RESUMEN

This report describes a headspace procedure suitable for the gas chromatographic assay of acetaldehyde, methanol, ethanol and various other volatile substances in biological samples. Carbopack B coated with 5% Carbowax 20-M is compared to Carbopack C coated with 0.2% Carbowax 1500. Assay range, linearity and precision are reported for the Carbopack B material.

MATERIALES
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Supelco
Tubo TD de acero inoxidable desactivado FLM Carbopack X, preconditioned, pkg of 10 tubes, O.D. × L 1/4 in. (6.35 mm) × 3 1/2 in. (89 mm)
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Metanol, analytical standard
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Adsorbente Carbopack, matrix Carbopack B, 60-80 mesh, bottle of 10 g
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Adsorbente Carbopack, matrix Carbopack C, 60-80 mesh, bottle of 10 g
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Adsorbente Carbopack, matrix Carbopack C, 80-100 mesh, bottle of 10 g
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Adsorbente Carbopack, matrix Carbopack X, 40-60 mesh, bottle of 10 g
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Carbopack B, O.D. × L 1/4 in. × 3 1/2 in., glass TD tube, fritted, Sealed with Brass Endcaps, preconditioned, pkg of 10 ea
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Adsorbente Carbopack, matrix Carbopack X, 60-80 mesh, bottle of 10 g
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Supelclean ENVI-Carb X, matrix Carbopack X, 120-400 mesh, bottle of 50 g
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Carbopack B, stainless steel TD tube, O.D. × L 1/4 × 3 1/2, unconditioned, pkg of 10 ea
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Carbopack X, glass TD tube, fritted, O.D. × L 1/4 in. × 3 1/2 in., preconditioned, pkg of 10 ea
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Carbopack B, glass TD tube, fritted, O.D. × L 1/4 in. × 3 1/2 in., preconditioned, pkg of 10 ea
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Carbopack B, glass TD tube, fritted, O.D. × L 1/4 in. × 3 1/2 in., unconditioned, pkg of 10 ea, matrix Carbopack
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Relleno de GC recubierto, phase 1% SP®-1510, matrix 60/80 Carbopack B support, bottle of 15 g