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Merck
  • Direct aerobic photo-oxidative synthesis of aromatic methyl esters from methyl aromatics via dimethyl acetals.

Direct aerobic photo-oxidative synthesis of aromatic methyl esters from methyl aromatics via dimethyl acetals.

Organic letters (2010-07-31)
Shin-Ichi Hirashima, Tomoya Nobuta, Norihiro Tada, Tsuyoshi Miura, Akichika Itoh
摘要

A useful method for facile synthesis of aromatic methyl esters from methyl aromatics via dimethyl acetals by aerobic photo-oxidation using inexpensive and easily handled CBr(4) as catalyst is reported. This is the first example for direct preparation of the corresponding aromatic methyl esters from methyl aromatics.

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Sigma-Aldrich
乙醛缩二甲醇, 95%
Sigma-Aldrich
1,1-二甲氧基乙烷, ≥97%, FG