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US EPA Method 8100: GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) on SPB®-608

US EPA Method 8100: GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) on SPB®-608 suitable for GC

Materials

analytical column

Product No.
Description
Pricing

SPB®-608 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.50 μm

SLB®-5ms Capillary GC Column

L × I.D. 20 m × 0.18 mm, df 0.18 μm

accessory

Product No.
Description
Pricing

Wheaton wide-mouth bottle

amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 ea

Supeltex M-2B Double-Tapered Ferrule

I.D. 0.4 mm, 0.10-0.25 mm to like I.D. Column, pkg of 2 ea

Capillary Column Butt Connector

body only (ferrules not included)

guard column

Product No.
Description
Pricing

Intermediate Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.25 mm

standard

Product No.
Description
Pricing

N-Nitrosodiphenylamine solution

certified reference material, 5000 μg/mL in methanol

Perfluorotributylamine (PFTBA)

analytical standard

EPA 8270 GC-MS Tuning Solution II

certified reference material, 1000 μg/mL each component in dichloromethane

EPA CLP Semivolatile Calibration Mix

certified reference material, 1000 μg/mL each component in dichloromethane : benzene (3:1)

EPA CLP Semivolatiles Surrogate Standards Mix

certified reference material, 4000 μg/mL each component in methylene chloride

EPA 8270 Semivolatile Internal Standard Mix

certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride, ampule of 2 × 1 mL

EPA 8270 Benzidines Mix

certified reference material, TraceCERT®, 2000 μg/mL each component in methanol, ampule of 1 mL

CONDITIONS

column

SPB-608, 30 m x 0.25 mm I.D., 0.25 μm (24103-U)

oven

80 °C (2 min), 15 °C/min to 250 °C, 8 °C/min to 300 °C (35 min)

inj. temp.

300 °C

MSD interface

300 °C

scan range

m/z 40 - 450

carrier gas

helium, 1.2 mL/min. constant

injection

0.5 μL, splitless (1 min)

sample

each analyte at 10 μg/mL in methylene chloride

Description

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany