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  • ortho-Acetoxylation of phosphonic and phosphoric monoacids via Pd(II) catalysis.

ortho-Acetoxylation of phosphonic and phosphoric monoacids via Pd(II) catalysis.

The Journal of organic chemistry (2013-08-07)
Li Yan Chan, Xiangjian Meng, Sunggak Kim
PMID23915334
ABSTRACT

A simple and efficient method is developed for Pd-catalyzed ortho-acetoxylation using organophosphates, namely, benzylic phosphonic and aryl phosphoric monoacids, as the directing group.

MATERIALS
Product Number
Brand
Product Description
438081
Sigma-Aldrich
Phosphoric acid, ACS reagent, ≥85 wt. % in H2O
Pricing and availability is not currently available.
79622
Sigma-Aldrich
Phosphoric acid, puriss. p.a., crystallized, ≥99.0% (T)
Pricing and availability is not currently available.