GC Analysis of Wieland-Miescher Ketone Enantiomers on Astec® CHIRALDEX™ G-TA
CONDITIONS
column
Astec CHIRALDEX G-TA, 30 m x 0.25 mm I.D., 0.12 μm (73033AST)
gradient
110 °C, 5 °C/min to 160 °C
inj. temp.
250 °C
detector
FID, 250 °C
carrier gas
helium, 35 psi
sample
peak 1: S(+)-Wieland-Miescher Ketone
peak 2: R(-)-Wieland-Miescher Ketone
Descripción
Analysis Note
Elution order reversal on CHIRALDEX G-BP.
Legal Information
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC