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224294

Sigma-Aldrich

Thiophosphoryl chloride

98%

Sinónimos:

Phosphorus sulfochloride, Phosphorus thiochloride

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About This Item

Fórmula lineal:
PSCl3
Número de CAS:
3982-91-0
Peso molecular:
169.40
EC Number:
223-622-6
MDL number:
MFCD00011504
UNSPSC Code:
12352100
PubChem Substance ID:
24853426
NACRES:
NA.22

assay

98%

form

liquid

refractive index

n20/D 1.555 (lit.)

bp

125 °C (lit.)

mp

−35 °C (lit.)

solubility

benzene: soluble(lit.)
carbon disulfide: soluble(lit.)
carbon tetrachloride: soluble(lit.)
chloroform: soluble(lit.)

density

1.668 g/mL at 25 °C (lit.)

SMILES string

ClP(Cl)(Cl)=S

InChI

1S/Cl3PS/c1-4(2,3)5

InChI key

WQYSXVGEZYESBR-UHFFFAOYSA-N

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Application

Thiophosphoryl chloride was used in the synthesis of O-ethyl dichlorothiophosphate.

pictograms

Skull and crossbonesCorrosion
GHS06,GHS05

signalword

Danger

Hazard Classifications

Acute Tox. 1 Inhalation - Acute Tox. 4 Oral - Eye Dam. 1 - Skin Corr. 1B - STOT SE 3

target_organs

Respiratory system

Storage Class

6.1B - Non-combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

wgk_germany

WGK 2

flash_point_f

Not applicable

flash_point_c

Not applicable

ppe

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

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Mohammed D Zidan et al.
Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 58(8), 1577-1582 (2002-08-09)
A new route has been devised, leading to the production of phosphorus thiotrihalides, SPX3 where X = F, Br and I by an on-line process using phosphorus thiotrichloride, SPCl3 as starting compound gassed over the following heated salts NaF, KBr
Wen Jun Gui et al.
Analytical biochemistry, 357(1), 9-14 (2006-08-22)
Two haptens of the insecticide triazophos (O,O-diethyl O-[1-phenyl-1H-1,2,4-triazol-3-yl] phosphorothioate) were synthesized by introducing appropriate spacers in the O-ethyl site of the analyte molecular structure. First, thiophosphoryl chloride (PSCl(3)) reacts with methanol at low temperature to give O-ethyl dichlorothiophosphate. After reacting
J T Slama et al.
Analytical biochemistry, 209(1), 143-149 (1993-02-15)
Elemental [35S]sulfur was shown to equilibrate with the sulfur of thiophosphoryl chloride when these materials are heated together. This isotopic exchange reaction is the basis of a convenient, microscale synthesis of high specific activity [35S]PSCl3. [35S]Thiophosphoryl chloride is otherwise not
Sarah E Lee et al.
Chembiochem : a European journal of chemical biology, 12(4), 633-640 (2011-02-10)
The elucidation of signalling pathways relies heavily upon the identification of protein kinase substrates. Recent investigations have demonstrated the efficacy of chemical genetics using ATP analogues and modified protein kinases for specific substrate labelling. Here we combine N(6) -(cyclohexyl)ATPγS with
[Hygienic substantiation of the maximum permissible level of phosphorus thiotrichloride in reservoir water].
V M Tomkiv
Gigiena i sanitariia, (11)(11), 68-70 (1988-11-01)
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