GC Analysis of Alcohol Enantiomers on β-DEX^™ 325

column

β-DEX 325, 30 m × 0.25 mm I.D., 0.25 μm (24308)

oven

110 °C, 1-phenyl-2-propanol; 100 °C, isopinocampheol; 90 °C, 6-methyl-5-hepten-2-ol

inj. temp.

220 °C

detector

FID, 300 °C

carrier gas

helium, 20 cm/sec @ analysis temperature

injection

1 μL 100:1 split

sample

1 mg/mL in methylene chloride