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Synthesis of gold nanoparticles with graphene oxide.

Journal of nanoscience and nanotechnology (2014-04-17)
Wenshuo Wang, Dawei He, Xiqing Zhang, Jiahua Duan, Hongpeng Wu, Haiteng Xu, Yongsheng Wang
ABSTRACT

Single sheets of functionalized graphene oxide are derived through chemical exfoliation of natural flake graphite. We present an effective synthetic method of graphene-gold nanoparticles hybrid nanocomposites. AFM (Atomic Force Microscope) was used to measure the thickness of the individual GO nanosheet. FTIR (Fourier transform infrared) spectroscopy was used to verify the attachment of oxygen functionalities on the surface of graphene oxide. TEM (Transmission Electron Microscope) data revealed the average diameters of the gold colloids and characterized the composite particles situation. Absorption spectroscopy showed that before and after synthesis the gold particle size did not change. Our studies indicate that the hybrid is potential substrates for catalysts and biosensors.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Graphite, powder, <20 μm, synthetic
Sigma-Aldrich
Graphite, flakes
Sigma-Aldrich
Graphite, powder, <45 μm, ≥99.99% trace metals basis
Sigma-Aldrich
Graphite, rod, L 150 mm, diam. 3 mm, low density, 99.995% trace metals basis
Sigma-Aldrich
Graphite, powder, <150 μm, 99.99% trace metals basis
Sigma-Aldrich
Graphite, rod, L 150 mm, diam. 6 mm, 99.995% trace metals basis