HPLC Analysis of Jacobsen Catalyst Enantiomers on Astec® CYCLOBOND I 2000 HP-RSP (TEA mobile phase)
Materiales
Analytical column
Referencia del producto
Descripción
Precios
Astec® Cyclobond I 2000 HP-RSP Chiral HPLC Column
5 μm particle size, L × I.D. 25 cm × 4.6 mmstandard
Referencia del producto
Descripción
Precios
(R,R)-(−)-N,N′-Bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminomanganese(III) chloride
(S,S)-(+)-N,N′-Bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminomanganese(III) chloride
CONDITIONS
column
CYCLOBOND I 2000 HP-RSP, 25 cm x 4.6 mm I.D., 5 μm particles (24024AST)
mobile phase
[A] acetonitrile; [B] methanol; [C] acetic acid; [D] triethylamine; (95:5:0.2:0.1, A:B:C:D)
column temp.
25 °C
flow rate
1.5 mL/min
detector
UV, 254 nm
injection
2 μL
sample
5 mg/mL in methanol
Descripción
Legal Information
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
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