Residual solvents in pharmaceutical preparations
Materiales
SPME fiber
Referencia del producto
Descripción
Precios
Filtro SPME Polidimetilsiloxano (PDMS)
df 100 μm(PDMS, needle size 24 ga, for use with manual holderCONDITIONS
SPME fiber
polydimethylsiloxane, 100 μm (57300-U)
extraction
headspace or immersion sampling (15 min) 1 min desorption
column
SPB-624, 75 m × 0.53 mm I.D., 3.0 μm (25432)
oven
40 °C (35 min) to 220 °C at 40 °C/min, hold 5 min
inj. temp.
splitless (closed 3 min), 200 °C
detector
FID, 250 °C
carrier gas
helium, 35 cm/sec
Descripción
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany