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Merck

Veterinary drug residues in domestic and imported foods of animal origin in the Republic of Korea.

Food additives & contaminants. Part B, Surveillance (2014-12-30)
JeongWoo Kang, Hae-Chul Park, Vinayakumar Gedi, Su-Jeong Park, Myeong-Ae Kim, Min-Kyoung Kim, Hyun-Jung Kwon, Byung-Hoon Cho, Tae-Wan Kim, Kwang-Jick Lee, Chae-Mi Lim
RESUMEN

The Korean National Residue Programme comprises three different approaches for evaluating domestic and imported foods of animal origin: monitoring, surveillance/enforcement and an exploratory test programme. Monitoring and surveillance/enforcement testing programmes are routinely implemented by 17 Provincial Veterinary Services for domestic products and regional offices of the Animal and Plant Quarantine Agency (QIA) for imported products. The exploratory project conducted at QIA headquarters is designed to test substances that are not included in monitoring and enforcement testing programmes. Here, we carried out exploratory testing for determining the presence of 42 veterinary drugs that have no established Korean maximum residue limits and analysed their levels simultaneously, in a total of 3108 samples of domestic and imported animal-origin foods. Of the tested drugs, acetylsalicylic, paracetamol, clopidol, diclazuril, amprolium, toltrazuril and its metabolites (toltrazuril sulphone and toltrazuril sulphoxide) and phenylbutazone and its metabolites (oxyphenylbutazone) were detected.

MATERIALES
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Dexametasona, powder, BioReagent, suitable for cell culture, ≥97%
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Acetonitrilo, anhydrous, 99.8%
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Dexametasona, ≥98% (HPLC), powder
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Acetylsalicylic acid, ≥99.0%
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Ácido acético, for luminescence, BioUltra, ≥99.5% (GC)
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Aspirin, meets USP testing specifications
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Ácido acético, ≥99.5%, FCC, FG
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Prednisona, ≥98%
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Prednisolone, ≥99%
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Ácido acético, natural, ≥99.5%, FG
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5α-Androstan-17β-ol-3-one, ≥97.5%
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Dexametasona, powder, γ-irradiated, BioXtra, suitable for cell culture, ≥80% (HPLC)
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Ethylene, ≥99.5%
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Acetylsalicylic acid, analytical standard
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Acetonitrilo, HPLC Plus, ≥99.9%, poly-coated bottles
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Acetonitrilo, electronic grade, 99.999% trace metals basis
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Acetonitrilo solution, contains 0.1 % (v/v) formic acid, suitable for HPLC
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Betamethasone, ≥98%
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Phenylbutazone
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Acetonitrilo solution, contains 0.1 % (v/v) trifluoroacetic acid, suitable for HPLC
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Ethylene, 99.99%
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Flumethasone
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Nicarbazin
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Dexametasona, meets USP testing specifications
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Amprolium hydrochloride
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Tolfenamic acid, NSAID
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Acetonitrilo, ≥99.5%, ACS reagent
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Acetic acid-12C2, 99.9 atom % 12C
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Acetonitrilo solution, contains 0.05 % (w/v) ammonium formate, 5 % (v/v) water, 0.1 % (v/v) formic acid, suitable for HPLC
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Acetonitrilo solution, contains 0.05 % (v/v) trifluoroacetic acid