24048
SPB®-5 Capillary GC Column
L × I.D. 30 m × 0.32 mm, df 0.25 μm
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About This Item
UNSPSC Code:
41115710
eCl@ss:
32119290
Recommended Products
material
fused silica
Agency
meets requirements for USP G27 and G36
parameter
-60-320 °C temperature (isothermal or programmed)
Beta value
320
df
0.25 μm
technique(s)
gas chromatography (GC): suitable
L × I.D.
30 m × 0.32 mm
matrix active group
Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase
column type
capillary non-polar
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General description
Application: This non-polar general purpose column provides primarily a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
USP Code: This column meets USP G27 and G36 requirements.
Phase:
- Bonded
- Poly(5% diphenyl/95% dimethyl siloxane)
- ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
- ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
- ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
- ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)
Application
SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may also be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. Furthermore, it may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.
Other Notes
We offer a variety of chromatography accessories including analytical syringes
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
Hazard Statements
Precautionary Statements
Hazard Classifications
Aquatic Chronic 2
Storage Class Code
13 - Non Combustible Solids
WGK
WGK 2
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
Determination of sterols by capillary column gas chromatography. Differentiation among different types of olive oil: virgin, refined, and solvent-extracted.
Jimenez O and Gonzalez ADV.
Journal of the American Oil Chemists' Society, 73 (12), 1685-1689 (1996)
J Corwin et al.
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Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
Chromatograms
suitable for GC, application for SPEOur team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.
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