- Synthesis of the beta-D-glucuronides of 2,3-, 3,4-, and 2,6-dichlorophenol.
Synthesis of the beta-D-glucuronides of 2,3-, 3,4-, and 2,6-dichlorophenol.
Archiv der Pharmazie (2001-04-24)
S Goenechea, G Rücker, M A Hubert
PMID11315335
RÉSUMÉ
The beta-D-glucuronides of 2,3-, 3,4-, and 2,6-dichlorophenol (1-3) were prepared by a modified Koenigs-Knorr synthesis. As the alkaline hydrolysis of perpivaloylated methyl (2,3-dichlorophenyl)-glucuronate 1a led to a dehydrated glucuronide, the preparation of peracetylated methyl dichlorophenylglucuronates with subsequent cleavage of the ester bindings under mild conditions was preferred.
MATÉRIAUX
Référence du produit
Marque
Description du produit
Référence
Conditionnement
Disponibilité
Prix
Quantité