Direkt zum Inhalt
Merck
  • One-step dispersion of cellulose nanofibers by mechanochemical esterification in an organic solvent.

One-step dispersion of cellulose nanofibers by mechanochemical esterification in an organic solvent.

ChemSusChem (2012-11-28)
Pei Huang, Min Wu, Shigenori Kuga, Deqian Wang, Dayong Wu, Yong Huang
ZUSAMMENFASSUNG

Got a crush: Native cellulose can be dispersed as nanofibers in organic solvents by ball milling with esterification agents. Milling with hexanoyl chloride/DMF gives hexanoyl-coated nanofibers dispersible in several organic solvents. Milling with succinic anhydride/DMSO results water-dispersible nanofibers. The results open the way to new cellulose mechanochemistries.

MATERIALIEN
Produktnummer
Marke
Produktbeschreibung

Sigma-Aldrich
N,N-Dimethylformamid, ACS reagent, ≥99.8%
Sigma-Aldrich
N,N-Dimethylformamid, suitable for HPLC, ≥99.9%
Sigma-Aldrich
N,N-Dimethylformamid, ReagentPlus®, ≥99%
Sigma-Aldrich
N,N-Dimethylformamid, for molecular biology, ≥99%
Sigma-Aldrich
N,N-Dimethylformamid, biotech. grade, ≥99.9%
Sigma-Aldrich
Hexanoylchlorid, 97%
Sigma-Aldrich
Hexanoylchlorid, ≥99%
Supelco
N,N-Dimethylformamid, analytical standard