콘텐츠로 건너뛰기
Merck
모든 사진(1)

문서

55227-U

Supelco

Supel QuE QuEChERS tube

Citrate Extraction Tube, pk of 50, suitable for EN 15662

동의어(들):

QuEChERS

로그인조직 및 계약 가격 보기


About This Item

UNSPSC 코드:
41115712
NACRES:
NB.21

product name

Supel QuE, Citrate Extraction Tube, pk of 50, suitable for EN 15662

material

polypropylene tube

Agency

suitable for EN 15662

제품 라인

Supel

구성

magnesium sulfate, 4 g
sodium chloride, 1 g (Cat. No. S7653)
sodium citrate dibasic sesquihydrate, 0.5 g (Cat. No. 71635)
sodium citrate tribasic dihydrate, 1 g (Cat. No. S4641)

포장

pk of 50

기술

QuEChERS: suitable

원심분리 튜브 용적

15 mL

응용 분야

food and beverages

분리 기술

ion exchange

유사한 제품을 찾으십니까? 방문 제품 비교 안내

일반 설명

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

애플리케이션

Supel QuE citrate tube is used for the determination of pesticide residues on vegetables using various analytical techniques.

적합성

Suitable for extracting ~10 g food/agricultural sample. The citrate is to buffer the extraction to pH 5.0 - 5.5. At this pH, most acid and base labile pesticides are stable.

법적 정보

Supel is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

13 - Non Combustible Solids

WGK

WGK 1

Flash Point (°F)

Not applicable

Flash Point (°C)

Not applicable


Choose from one of the most recent versions:

시험 성적서(COA)

Lot/Batch Number

Don't see the Right Version?

If you require a particular version, you can look up a specific certificate by the Lot or Batch number.

이 제품을 이미 가지고 계십니까?

문서 라이브러리에서 최근에 구매한 제품에 대한 문서를 찾아보세요.

문서 라이브러리 방문

이미 열람한 고객

Monitoring survey of the use patterns and pesticide residues on vegetables in the Niayes zone, Senegal
Diop A, et al.
Chemosphere, 144, 1715-1721 (2016)
Pesticide analysis at ppt concentration levels: coupling nano-liquid chromatography with dielectric barrier discharge ionization-mass spectrometry
Mirabelli.FM, et al.
Analytical and Bioanalytical Chemistry, 408(13), 3425-3434 (2016)
Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
Yelena Sapozhnikova et al.
Analytica chimica acta, 758, 80-92 (2012-12-19)
A multi-class, multi-residue method for the analysis of 13 novel flame retardants, 18 representative pesticides, 14 polychlorinated biphenyl (PCB) congeners, 16 polycyclic aromatic hydrocarbons (PAHs), and 7 polybrominated diphenyl ether (PBDE) congeners in catfish muscle was developed and evaluated using

문서

Pistachios 45% fat complicates pesticide analysis. But Z-Sep+ sorbent cleanup after QuEChERS extraction can reduce background for reliable results.

Dual-layer cartridge achieves efficient SPE clean-up for challenging pesticide residue testing in turmeric and spices.

2-layer SPE cartridge efficiently reduces background for ginger contaminant analysis.

프로토콜

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

관련 콘텐츠

QuEChERS는 ‘Quick, Easy, Cheap, Effective, Rugged, Safe’ 시료 정화 방법으로 살충제 분석을 위해 식품과 농산물 시료 전처리에 사용합니다. QuEChERS는 시료 전처리에서 고체상 추출법(SPE) 기술에 기반합니다.

QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.

고체상 추출법(SPE)은 크로마토그래피 분석(예: HPLC, GC, TLC)에 앞서 빠르고 선택적인 시료 전처리 및 정제에 사용되는 기법입니다. SPE는 데이터를 개선하고 분석용 컬럼을 보호하기 위하여 시료 매트릭스를 교환하고, 분석물을 농축하며, 간섭과 오염 물질을 제거하는 데 사용됩니다.

Solid phase extraction purifies samples for chromatographic analysis, improving data quality and protecting analytical columns.

Chromatograms

application for HPLCapplication for HPLC, application for SPE

자사의 과학자팀은 생명 과학, 재료 과학, 화학 합성, 크로마토그래피, 분석 및 기타 많은 영역을 포함한 모든 과학 분야에 경험이 있습니다..

고객지원팀으로 연락바랍니다.