GCによる 1-フェニルエチルアミンエナンチオマー(N-トリフルオロアセチル誘導体)の分析、Astec® CHIRALDEX™ B-DM
材料
分析カラム
製品番号
詳細
価格
CONDITIONS
column
Astec CHIRALDEX B-DM, 30 m x 0.25 mm I.D., 0.12 μm (77023AST)
oven
120 °C
inj. temp.
250 °C
detector
FID, 250 °C
carrier gas
helium, 30 psi
injection
1 μL, 80:1 split
sample
3 mg/mL in methylene chloride
peak 1: R(+)-1-phenylethylamine (N-TFA derivative)
peak 2: S(-)-1-phenylethylamine (N-TFA derivative)
詳細
アナリシスノート
Can reverse elution order by using N-acetyl derivative on CHIRALDEX B-DM and B-PM, the N-chloroacetyl derivative on B-PM, or the N-TFA derivative on B-PH.
法的情報
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC