US EPA Method TO-17: GC Analysis of Volatiles on VOCOL after Collection/Desorption using Carbotrap® 300 Tube
Materiales
Analytical column
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related product
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Carbotrap® 300
glass TD tube, fritted, O.D. × I.D. × L 6 mm × 4 mm × 7 in., preconditioned, pkg of 1 eastandard
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CONDITIONS
sample/matrix
JHAP-43 Gas Mix (500429), 1ppm each component, 20mL
adsorbent tube
Carbotrap 300 (28283-U)
desorption process
20 mL/min at 330 °C for 6 min (cryo-focused to inlet @ -150°C)
column
SPB-1, 60 m × 0.25 mm I.D., 3.0 μm
oven
35°C (8 min), 5°C/min to 100°C (0 min), 15°C/min to 230°C (8 min)
detector
MSD, scan range 35-269
carrier gas
helium 31cm/sec
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Legal Information
Carbotrap is a registered trademark of Merck KGaA, Darmstadt, Germany