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  • Stability of canola oil encapsulated by co-extrusion technology: effect of quercetin addition to alginate shell or oil core.

Stability of canola oil encapsulated by co-extrusion technology: effect of quercetin addition to alginate shell or oil core.

Food chemistry (2013-09-05)
Geoffrey I N Waterhouse, Wei Wang, Dongxiao Sun-Waterhouse
ABSTRACT

This study examines the co-extrusion encapsulation of canola oil by alginate, with an antioxidant (quercetin) incorporated either in the oil core or alginate shell. Optical and environmental scanning electron microscopy revealed spherical beads of diameter ∼350μm and wall thickness ∼65μm. Bead appearance, size, wall thickness and surface characteristics did not change appreciably after treatments at pH 3 for 2h, pH 6.5 for 2h or pH 6.5 for 1min then pH 3 for 2h, although the amounts of phenolics released from beads differed depending on the conditions. The quercetin addition approach strongly influenced the stability of canola oil during storage at 20 and 38°C. Quercetin in the core more effectively suppressed oil deterioration. Quercetin in shell caused a higher phenolic content after storage. FTIR and HPLC analyses were used to track changes in the chemical composition of the encapsulated oil beads during storage.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Quercetin, ≥95% (HPLC), solid
Sigma-Aldrich
Alginic acid sodium salt from brown algae, BioReagent, suitable for immobilization of micro-organisms
Sigma-Aldrich
Alginic acid sodium salt, powder
Supelco
Canola oil, analytical standard
Sigma-Aldrich
Alginic acid calcium salt from brown algae
Sigma-Aldrich
Alginic acid sodium salt from brown algae, Medium viscosity
Sigma-Aldrich
Alginic acid sodium salt from brown algae, low viscosity
Sigma-Aldrich
Sodium alginate
Sigma-Aldrich
Alginic acid from brown algae, powder