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[Research on chemical constituents from stem of Gymnema sylvestre].

Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials (2008-12-31)
Han-shen Zhen, Xue-yan Zhu, Ru-mei Lu, Jie Liang, Qin Qiu, Qi-miao Meng
ABSTRACT

To study on the chemical constituents from the stem of Gymnema sylvestre. The constituents were extracted by percolation with ethanol. Then the extract was separated by systemic solvent separation methods. The part of n-butanol extract was isolated and purified by macroporous adsorptive resins, silica gel column chromatography, sephadex gel column chromatography and recrystallization. The isolated compounds were identified by spectrum methods. Eight compounds were isolated and identified as fallows: Conduritol A(I), 1-Heptadecanol(II), Stigmasterol glucoside(III), 1-Quercitol(IV), 1-Octadecanol(V), Potassium nitrate(VI), Lupeol cinnamate(VII), Stigmasterol(VIII). Chemical compounds II, III, V, VII are firstly obtained from this plant.

MATERIALS
Product Number
Brand
Product Description

Stearyl alcohol, European Pharmacopoeia (EP) Reference Standard
Supelco
Stearyl Alcohol, Pharmaceutical Secondary Standard; Certified Reference Material
Sigma-Aldrich
1-Octadecanol, 95%
Supelco
1-Octadecanol, Selectophore, ≥99.0%
Sigma-Aldrich
1-Octadecanol, ReagentPlus®, 99%