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GC Analysis of Residual Solvents on SPB®-624 after SPME using 100 μm PDMS Fiber

GC Analysis of Residual Solvents on SPB®-624 after SPME using 100 μm PDMS Fiber suitable for GC, application for SPME

Materials

SPME fiber

Product No.
Description
Pricing

SPME fiber assembly Polydimethylsiloxane (PDMS)

df 100 μm(PDMS, needle size 24 ga, for use with manual holder

CONDITIONS

SPME fiber

polydimethylsiloxane, 100 μm (57300-U)

extraction

headspace or immersion sampling (15 min) 1 min desorption

column

SPB-624, 75 m × 0.53 mm I.D., 3.0 μm (25432)

oven

40 °C (35 min) to 220 °C at 40 °C/min, hold 5 min

inj. temp.

splitless (closed 3 min), 200 °C

detector

FID, 250 °C

carrier gas

helium, 35 cm/sec

Description

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany