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25420-U

Supelco

SPB®-5 Capillary GC Column

L × I.D. 30 m × 0.53 mm, df 1.00 μm

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About This Item

UNSPSC Code:
12000000
eCl@ss:
32119290
NACRES:
SB.54

material

fused silica

Agency

meets requirements for USP G27 and G36

parameter

-60-300 °C temperature (isothermal)
-60-320 °C temperature (programmed)

Beta value

133

df

1.00 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.53 mm

matrix active group

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

column type

capillary non-polar

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General description

Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.
Application: This non-polar general purpose column provides primarily a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded
  • Poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
  • ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
  • ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
  • ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)

Application

SPB®-5 Capillary GC Column may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
Determination of sterols by capillary column gas chromatography. Differentiation among different types of olive oil: virgin, refined, and solvent-extracted.
Jimenez O and Gonzalez ADV.
Journal of the American Oil Chemists' Society, 73 (12), 1685-1689 (1996)
P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
J Corwin et al.
Cancer, 43(3), 1007-1013 (1979-03-01)
Solitary plasmacytoma of bone (SPB) and extramedullary plasmacytoma (EMPC) are unusual solitary tumors of plasma cell origin. The clinical differences between these tumors and multiple myeloma are the subject of continued study. This review examines the radiotherapy experience at M.
H J Chou
Journal of AOAC International, 81(5), 943-947 (1998-10-17)
Diethanolamine (DEA) is a precursor of N-nitrosodiethanolamine (NDELA), an animal carcinogen. A gas chromatographic (GC) method was developed for determining DEA in fatty acid diethanolamides that are commonly used in cosmetic products. Methanolic solutions of the amides were analyzed by

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