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  • Determination of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio using modified QuEChERS combined with liquid chromatography-tandem mass spectrometry.

Determination of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio using modified QuEChERS combined with liquid chromatography-tandem mass spectrometry.

Food chemistry (2017-09-28)
Mohammad Faraji, Roya Noorbakhsh, Hooshang Shafieyan, Mohammadkazem Ramezani
RÉSUMÉ

A QuEChERS based methodology was developed for the simultaneous identification and quantification of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio by liquid chromatography-tandem mass spectrometry for the first time. First, sample extraction was done with MeCN:citrate buffer:NaHCO

MATÉRIAUX
Référence du produit
Marque
Description du produit

Supelco
Supel QuE, Citrate/Sodium Bicarbonate Tube, pk of 50
Supelco
Imidacloprid-d4, PESTANAL®, analytical standard
Supelco
Spirotetramat, PESTANAL®, analytical standard
Supelco
N-(6-Chloro-3-pyridylmethyl)-N′-cyano-acetamidine, PESTANAL®, analytical standard