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Merck

Comparative evaluation of determination of beta-lactam intermediates.

Hindustan antibiotics bulletin (1993-08-01)
B S Deshpande, S S Ambedkar, J G Shewale
ZUSAMMENFASSUNG

The Schiff's base formation between 6-aminopenicillanic acid, 7-aminodesacetoxycephalosporanic acid and 7-aminocephalosporanic acid and p-dimethylaminobenzaldehyde (PDAB) was investigated. The factors that affect the reaction such as concentration of PDAB, time and pH were studied and optimised for estimation of these intermediates.

MATERIALIEN
Produktnummer
Marke
Produktbeschreibung

Sigma-Aldrich
4-(Dimethylamino)benzaldehyd, 98%
Sigma-Aldrich
4-(Dimethylamino)benzaldehyd, suitable for histochemical demonstration of nitro blue tetrazolium reduction in neutrophils
Sigma-Aldrich
4-(Dimethylamino)benzaldehyd, ACS reagent, 99%
Millipore
Kovac-Reagenz für Indole, suitable for microbiology
Millipore
Kovac-Reagenz für Indole, suitable for microbiology
Sigma-Aldrich
4-(Dimethylamino)benzaldehyd, puriss. p.a., reag. Ph. Eur., ≥99% (perchloric acid titration)
Supelco
4-Dimethylamino-benzaldehyd -Lösung, 10 g/L in isopropanol, for TLC derivatization