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  • LiBF4-mediated C-glycosylation of glycals with allyltrimethylsilane: a facile synthesis of allyl C-glycosylic compounds.

LiBF4-mediated C-glycosylation of glycals with allyltrimethylsilane: a facile synthesis of allyl C-glycosylic compounds.

Carbohydrate research (2001-07-04)
J S Yadav, B V Reddy, L Chandraiah, K S Reddy
ZUSAMMENFASSUNG

The treatment of glycals with allyltrimethylsilane in the presence of lithium tetrafluoroborate in acetonitrile gave the corresponding allyl 2,3-unsaturated C-glycosylic compounds in excellent yields with high anomeric selectivity.

MATERIALIEN
Produktnummer
Marke
Produktbeschreibung

Sigma-Aldrich
Lithiumfluorborat, 98%
Sigma-Aldrich
Allyltrimethylsilan, 98%
Sigma-Aldrich
Lithiumfluorborat, ultra dry, powder, 99.99% trace metals basis
Sigma-Aldrich
Tri-O-acetyl-D-glucal, 98%