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  • Synthesis and characterization of N,N-dimethyldodecylamine-capped Aucore-Pdshell nanoparticles in toluene.

Synthesis and characterization of N,N-dimethyldodecylamine-capped Aucore-Pdshell nanoparticles in toluene.

Langmuir : the ACS journal of surfaces and colloids (2005-11-03)
Sudip Nath, Snigdhamayee Praharaj, Sudipa Panigrahi, Sujit Kumar Ghosh, Subrata Kundu, Soumen Basu, Tarasankar Pal
ABSTRACT

In this paper a convenient route for synthesizing Au(core)-Pd(shell) bimetallic nanoparticles in toluene has been reported as a result of co-reduction of gold(III) and palladium(II) precursors in toluene. N,N-Dimethyldodecylamine was used as a capping agent for the core-shell particles, which not only imparts stability to the organosol but also controls morphology of the evolved particles. The particles were characterized using UV-visible, transmission electron microscopy, and X-ray diffraction measurements. All results substantiate the formation of core-shell structure of the synthesized particles.

MATERIALS
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Sigma-Aldrich
N,N-Dimethyldodecylamine, 97%