- Large dose hyperpolarized water with dissolution-DNP at high magnetic field.
Large dose hyperpolarized water with dissolution-DNP at high magnetic field.
Journal of magnetic resonance (San Diego, Calif. : 1997) (2016-11-28)
Kasper Wigh Lipsø, Sean Bowen, Oleksandr Rybalko, Jan Henrik Ardenkjær-Larsen
PMID27889650
RÉSUMÉ
We demonstrate a method for the preparation of hyperpolarized water by dissolution Dynamic Nuclear Polarization at high magnetic field. Protons were polarized at 6.7T and 1.1K to >70% with frequency modulated microwave irradiation at 188GHz. 97.2±0.7% of the radical was extracted from the sample in the dissolution in a two-phase system. 16±1mL of 5.0M
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