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LC/MS Analysis of 2C Amines Drugs of Abuse on Ascentis® Express HILIC

LC/MS Analysis of 2C Amines Drugs of Abuse on Ascentis® Express HILIC application for HPLC

Materials

analytical column

Product No.
Description
Pricing

53939-U

Ascentis® Express HILIC, 2.7 μm HPLC Column

2.7 μm particle size, L × I.D. 10 cm × 2.1 mm

mobile phase component

Product No.
Description
Pricing

70221

Ammonium formate

eluent additive for LC-MS, LiChropur™, ≥99.0%

standard

Product No.
Description
Pricing

B-026

4-Bromo-2,5-dimethoxyphenethylamine hydrochloride solution

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

C-122

2C-B-FLY hydrochloride solution

1 mg/mL in acetonitrile: water (9:1), ampule of 1 mL, certified reference material, Cerilliant®

CONDITIONS

column

Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U)

mobile phase

5 mM ammonium formate in acetonitrile:water (90:10, v/v)

flow rate

0.4 mL/min

column temp.

35 °C

detector

TOF/MS

detector

2.0 μL

sample

300 ng/mL in acetonitrile

Description

Legal Information

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

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Small Molecule HPLCLarge Molecule HPLCGas Chromatography (GC)TLCSolid Phase Microextraction (SPME)Solid Phase Extraction (SPE)QuEChERS