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  • Convergent synthesis of trifunctional molecules by three sequential azido-type-selective cycloadditions.

Convergent synthesis of trifunctional molecules by three sequential azido-type-selective cycloadditions.

Chemical communications (Cambridge, England) (2018-03-13)
Suguru Yoshida, Kimiyuki Kanno, Isao Kii, Yoshihiro Misawa, Masatoshi Hagiwara, Takamitsu Hosoya
ABSTRACT

A facile strategy for the synthesis of trifunctional molecules involving three sequential selective triazole-forming reactions is proposed. This method exploits three kinds of mechanistically different azido-type-selective cycloadditions. Three different azidophiles could be efficiently connected to a triazido platform molecule with three types of azido groups in a consecutive manner, which rendered a practical trifunctional molecule readily available.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
1-Biotinyl-3,6-dioxa-8-octaneamine hydrochloride, ≥95%
Sigma-Aldrich
5-(Biotinamido)pentylamine TFA Salt, ≥95%