21104
GC Stationary Phase
phase OV-1, bottle of 10 g
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About This Item
Produtos recomendados
Agency
meets requirements for USP G2
embalagem
bottle of 10 g
Parâmetros
100-350 °C temp. range
técnica(s)
gas chromatography (GC): suitable
Grupo ativo da matriz
OV-1 phase
solubilidade
chloroform, toluene: soluble
tipo de coluna
packed GC
Descrição geral
GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are a few parameters that should be considered before choosing a stationary phase. OV-1 is suitable for the separation of drugs, alkaloids, phenols and steroids.
Synthesized specifically to be purer, of narrow molecular weight range, and without trace catalysts or impurities for use as a GC stationary phase.
Aplicação
OV-1 is suitable as stationary phase for monitoring the urinary excretion in man for pentachlorophenol (PCP) and PCP conjugated to glucuronic acid using gas chromatography with electron capture detection (GC/ECD).
Código de classe de armazenamento
10 - Combustible liquids
Classe de risco de água (WGK)
WGK 1
Ponto de fulgor (°F)
214.0 °F - closed cup
Ponto de fulgor (°C)
101.1 °C - closed cup
Equipamento de proteção individual
Eyeshields, Gloves
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Archives of toxicology, 58(3), 182-186 (1986-02-01)
Pentachlorophenol (PCP) was given orally to three volunteers at single doses of 3.9, 4.5, 9, and 18.8 mg. Daily urinary excretion of PCP and PCP conjugated to glucuronic acid was monitored using gas chromatography with electron capture detection (GC/ECD). Based
Remington: The Science and Practice of Pharmacy, 605-605 (2006)
Methods of Air Sampling and Analysis, 98-98 (1988)
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