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  • Microwave-assisted synthesis of salicylamide via BCl3 mediated coupling.

Microwave-assisted synthesis of salicylamide via BCl3 mediated coupling.

Journal of combinatorial chemistry (2005-07-12)
Lei Zhang, John Y Zhang
ABSTRACT

A novel and efficient microwave-assisted, BCl3-mediated coupling reaction to synthesize salicylamide structures from phenols and isocyanates is described.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Boron trichloride solution, 1.0 M in toluene
Sigma-Aldrich
Boron trichloride solution, 1.0 M in methylene chloride
Sigma-Aldrich
Boron trichloride solution, 1.0 M in heptane
Sigma-Aldrich
Boron trichloride solution, 1.0 M in p-xylene