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  • Evaluation of bi-functionalized mesoporous silicas as reversed phase/cation-exchange mixed-mode sorbents for multi-residue solid phase extraction of veterinary drug residues in meat samples.

Evaluation of bi-functionalized mesoporous silicas as reversed phase/cation-exchange mixed-mode sorbents for multi-residue solid phase extraction of veterinary drug residues in meat samples.

Talanta (2017-02-06)
Natalia Casado, Damián Pérez-Quintanilla, Sonia Morante-Zarcero, Isabel Sierra
ABSTRACT

A SBA-15 type mesoporous silica was synthesized and bi-functionalized with octadecylsilane (C18) or octylsilane (C8), and sulfonic acid (SO

MATERIALS
Product Number
Brand
Product Description

Supelco
Cimaterol, VETRANAL®, analytical standard
Supelco
Tulobuterol hydrochloride, VETRANAL®, analytical standard
Supelco
Carazolol, analytical standard
Sigma-Aldrich
Chloro(dimethyl)octylsilane, 97%
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Brombuterol hydrochloride, VETRANAL®, analytical standard
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Mabuterol hydrochloride, VETRANAL®, analytical standard
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Flunixin, VETRANAL®, analytical standard
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Clenproperol, VETRANAL®, analytical standard
Sigma-Aldrich
(3-Mercaptopropyl)triethoxysilane, ≥80% (GC), technical