Microwave-assisted synthesis of salicylamide via BCl3 mediated coupling.

Microwave-assisted synthesis of salicylamide via BCl3 mediated coupling.

Journal of combinatorial chemistry (2005-07-12)

Lei Zhang, John Y Zhang

RÉSUMÉ

A novel and efficient microwave-assisted, BCl3-mediated coupling reaction to synthesize salicylamide structures from phenols and isocyanates is described.

MATÉRIAUX

Référence du produit

Marque

Description du produit

178934

Sigma-Aldrich

Boron trichloride solution, 1.0 M in methylene chloride

348325

Sigma-Aldrich

Boron trichloride solution, 1.0 M in heptane

678732

Sigma-Aldrich

Boron trichloride, 1.0 M solution in toluene, 1.0 M in toluene

345458

Sigma-Aldrich

Boron trichloride solution, 1.0 M in p-xylene