UHPLC/MS Analysis of Heroin and Related Compounds on Titan C18
Materials
standard
Product No.
Description
Pricing
Alprazolam solution
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®Flunitrazepam solution
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®Heroin solution
1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®Morphine solution
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Titan C18 5 cm x 2.1 mm I.D., 1.9 μm particles (577122-U)
mobile phase
[A] 5 mM ammonium acetate in 95:5, water:acetonitrile; [B] 5 mM ammonium acetate in 5:95, water:acetonitrile
gradient
0 to 100% B in 3 min, held at 100% B for 1 min
flow rate
0.6 mL/min
pressure
6770 psi (467 bar)
column temp.
35 °C
detector
MS-TOF, XIC
injection
0.5 μL
sample
1 μg/mL in 95:5, water:methanol
Description
Analysis Note
This method shows heroin and related compounds separated on a Titan C18 column and MS detection. The highest quality LC-MS solvents were used to supply low background interference and low particulate contaminants for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.
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