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Total synthesis of broussonetine F: the orthoamide Overman rearrangement of an allylic diol.

Organic letters (2011-01-05)
Naoto Hama, Toshihiro Aoki, Shohei Miwa, Miki Yamazaki, Takaaki Sato, Noritaka Chida
ZUSAMMENFASSUNG

A first total synthesis of broussonetine F from diethyl L-tartrate was achieved. The cornerstone of our synthesis was an orthoamide Overman rearrangement, which provided an allylic amino alcohol with complete diastereoselectivity.

MATERIALIEN
Produktnummer
Marke
Produktbeschreibung

Sigma-Aldrich
(+)-Diethyl L-tartrat, ≥99%
Sigma-Aldrich
(−)-Diethyl-D-tartrat, ≥99%
Sigma-Aldrich
Diethyl L-tartrat, ≥99%, FG