LC/MS Analysis of Fluoroamphetamine Drugs of Abuse on Ascentis® Express HILIC
Materials
analytical column
Product No.
Description
Pricing
mobile phase component
Product No.
Description
Pricing
standard
Product No.
Description
Pricing
4-Fluoroamphetamine hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®(±)-2-Fluoroamphetamine hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®(±)-4-Fluoromethamphetamine hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®(±)-2-Fluoromethamphetamine hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U)
gradient
5 mM ammonium formate in acetonitrile:water (90:10, v/v)
flow rate
0.4 mL/min
column temp.
35 °C
detector
TOF/MS
injection
2 μL
sample
300 ng/mL in acetonitrile
Description
Analysis Note
The fluoroamphetamines (FA) are a group of "designer" stimulant drugs in amphetamine family. The rapid LC/MS analysis of four members of the FA family on Ascentis Express HILIC is shown here. Cerilliant CRMs were used to ensure reliable MS identification and quantification.
Legal Information
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany