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25467

Supelco

Carboxen®-1010 PLOT Capillary GC Column

Carboxen®-1010 PLOT Capillary GC Column

L × I.D. 30 m × 0.53 mm, average thickness 30 μm

Synonym(s):

Carboxen® 1010 PLOT Column, 30m x 0.53mm

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About This Item

EC Number:
262-373-8
UNSPSC Code:
41115710
eCl@ss:
32119290
Pricing and availability is not currently available.

material

fused silica

Quality Level

100

Agency

ASTM® D3612-96

description

PLOT = Porous Layer Open Tubular

manufacturer/tradename

Carboxen®

parameter

≤25-250 °C temperature (isothermal or programmed)

average thickness

30 μm

df

30 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.53 mm

matrix active group

Carbon molecular sieve phase

application(s)

chemicals and industrial polymers
food and beverages

column type

capillary PLOT

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General description

Application: This column is ideal for the separation of all major components in permanent gas (helium, hydrogen, oxygen, nitrogen, carbon monoxide, methane, and carbon dioxide) and light hydrocarbons (C2-C3) in the same analysis. It is the only column commercially available that is able to separate all major components in permanent gas. This column can also separate oxygen from nitrogen at subambient temperatures.
USP Code: None
Phase:
  • Carbon molecular sieve
Temp. Limits:
  • Subambient to 250 °C (isothermal or programmed)
Carboxen® Adsorbent is ideally used for solid-phase microextraction (SPME)[1] and does highly efficient extraction of small polar molecules from aqueous solution.[2] Porous-layer open-tubular (PLOT) columns are a powerful tool employed in gas chromatography during analysis of fixed gases, light hydrocarbons and volatile solvents. They are mostly preferred over traditional packed columns.[3]

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

ASTM is a registered trademark of American Society for Testing and Materials
Carboxen is a registered trademark of Merck KGaA, Darmstadt, Germany

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Certificates of Analysis (COA)

Lot/Batch Number
293452-08
293452-07
293452-06
293452-05
293452-04

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Applications of Solid Phase Microextraction
Pawliszyn J.
Applications of Solid Phase Microextraction, 64-65 (1999)
Porous layer open-tubular capillary columns: preparations, applications and future directions.
Zhenghua Ji
Journal of Chromatography A, 842 (1), 115-142 (1999)
Louise Urruty et al.
Journal of agricultural and food chemistry, 50(11), 3129-3136 (2002-05-16)
To provide an efficient and running analytical tool to strawberry plant breeders who have to characterize and compare the aromatic properties of new cultivars to those already known, a HS-SPME/GC-MS analysis method has been coupled with a statistical treatment method
Noushin Rastkari et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 877(14-15), 1568-1574 (2009-04-28)
Carbon nanotubes (CNTs) are a kind of new carbon-based nano-materials which have drawn great attention in many application fields. The potential single-walled carbon nanotubes (SWCNTs) as solid-phase microextraction (SPME) adsorbents for the preconcentration of environmental pollutants have been investigated in
B D Page et al.
Journal of chromatography. A, 873(1), 79-94 (2000-04-11)
The headspace solid-phase microextraction (HS-SPME) efficiencies from vegetable oil of the recently available Carboxen-poly(dimethylsiloxane) (PDMS) and divinylbenzene-Carboxen-PDMS fibres were found to be much greater than those of the PDMS fibre for a number of volatile contaminants. Using these Carboxen-based fibres
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Chromatograms

suitable for GC
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Questions

1–9 of 9 Questions  

  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer

    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

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  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer

    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

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  3. What are the specific functional groups that may affect the separation and the carbon saturated/unsaturated ratio of the material used in the Carboxen 1010 PLOT capillary column?

    1 answer

    1. The material used in the Carboxen 1010 PLOT capillary column does not retain any functional groups after the synthesis process due to the high temperatures involved. The carbon surface consists mainly of carbon and hydrogen, with very few exceptions.

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  4. Are there specific installation instructions available for the Carboxen-1010 plot column 24246, particularly regarding whether it needs to be baked out before use?

    1 answer

    1. The installation of capillary columns can differ based on the gas chromatography brand, detector type, injection port, and insertion distance. It's advisable to consult the GC manual for column insertion distance information and any special adapters required before installation.

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  5. Is the Carboxen 1010 PLOT column, Product 25467, GC/MS compatible?

    1 answer

    1. Yes, the particles are very strongly adhered to the surface of the column and would be compatible with mass spec detection.

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  6. What is the film thickness of the Carboxen™-1010 PLOT Capillary GC Column, Product 25467?

    1 answer

    1. The film thickness for this column is 30um.  The term "film" is somewhat of a misnomer because it is actually a layer of solid carboxen particles adhered to the fused silica tubing.

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  7. How can I purchase a column that is packed with this material?

    1 answer

    1. Most packed column are custom made and require that you obtain a quotation. Please contact our Customer & Sales Services group at phone number (800)-247-6628, fax number (800)-447-3044 or email [email protected] for additional information.

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  8. What types of compounds would be suitable for analysis on the Carboxen™-1010 PLOT Capillary GC Column, Product 25467?

    1 answer

    1. This column is designed for the analysis of permanent gases and light hydrocarbons up to a maximum of 3 carbon units.

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  9. What is the Department of Transportation shipping information for this product?

    1 answer

    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

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Reviews

Active Filters

  1. Sydney, Australia
    • Review 1
    • Votes 0
    5 out of 5 stars.

    Carboxen®-1010 PLOT Capillary GC Column

    Having used another similar column (different manufacturer) for the separation of H2, CO, CO2 and ethylene, I find this column to exhibit very good stability and reliability. Certainly, the high operational temperature rating is most welcomed.

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