663727
2,2,2-Trichloroethoxysulfonamide
97%
Synonym(s):
2,2,2-Trichloroethyl sulfamate, Sulfamic acid, 2,2,2-trichloroethyl ester
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All Photos(3)
About This Item
Empirical Formula (Hill Notation):
C2H4Cl3NO3S
CAS Number:
Molecular Weight:
228.48
MDL number:
UNSPSC Code:
12352100
PubChem Substance ID:
NACRES:
NA.22
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Assay
97%
form
solid
mp
52-58 °C
SMILES string
NS(=O)(=O)OCC(Cl)(Cl)Cl
InChI
1S/C2H4Cl3NO3S/c3-2(4,5)1-9-10(6,7)8/h1H2,(H2,6,7,8)
InChI key
VOKONKGVTXWZJI-UHFFFAOYSA-N
Gene Information
human ... STS(412)
Related Categories
Application
Nitrogen source in an intermolecular rhodium-catalyzed (662623) amination of C-H bonds.
Storage Class Code
11 - Combustible Solids
WGK
WGK 2
Flash Point(F)
>230.0 °F - closed cup
Flash Point(C)
> 110 °C - closed cup
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
Certificates of Analysis (COA)
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Kristin Williams Fiori et al.
Journal of the American Chemical Society, 129(3), 562-568 (2007-01-18)
Reaction methodology for intermolecular C-H amination of benzylic and 3 degrees C-H bonds is described. This process uses the starting alkane as the limiting reagent, gives optically pure tetrasubstituted amines through stereospecific insertion into enantiomeric 3 degrees centers, displays high
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