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455725

Sigma-Aldrich

N,N-Diisopropylbenzamide

98%

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About This Item

Linear Formula:
C6H5CON[CH(CH3)2]2
CAS Number:
20383-28-2
Molecular Weight:
205.30
MDL number:
MFCD00026370
UNSPSC Code:
12352100
PubChem Substance ID:
24868590

assay

98%

mp

69-71 °C (lit.)

SMILES string

CC(C)N(C(C)C)C(=O)c1ccccc1

InChI

1S/C13H19NO/c1-10(2)14(11(3)4)13(15)12-8-6-5-7-9-12/h5-11H,1-4H3

InChI key

UYXMMJPYFKRKKM-UHFFFAOYSA-N

Storage Class

13 - Non Combustible Solids

wgk_germany

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

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Certificates of Analysis (COA)

Lot/Batch Number
MKBQ7670V
MKBJ3394
65096TJ
10323AB
03806LI

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Naphthalene-catalysed lithiation of N,N-diisopropylbenzamide and its methoxy derivatives.
Alonso E, et al.
Tetrahedron, 54(44), 13629-13638 (1998)
Victoria L Blair et al.
Chemistry (Weinheim an der Bergstrasse, Germany), 14(1), 65-72 (2007-11-23)
Extending the recently introduced concept of "alkali-metal-mediated manganation" to functionalised arenes, the heteroleptic sodium manganate reagent [(tmeda)Na(tmp)(R)Mn(tmp)] (1; TMEDA=N,N,N',N'-tetramethylethylenediamine, TMP=2,2,6,6-tetramethylpiperidide, R=CH2SiMe3) has been treated with anisole or N,N-diisopropylbenzamide in a 1:1 stoichiometry in hexane. These reactions afforded the crystalline products
2-azaisobenzofurans as intermediates in a convenient annelation of aromatic tertiary amides.
Beak P and Chen C-W.
Tetrahedron Letters, 24(29), 2945-2948 (1983)

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