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assay
98%
form
liquid
refractive index
n20/D 1.51 (lit.)
bp
73-74 °C/47 mmHg (lit.)
density
1.767 g/mL at 25 °C (lit.)
functional group
bromo
SMILES string
C[C@H](Br)[C@@H](C)Br
InChI
1S/C4H8Br2/c1-3(5)4(2)6/h3-4H,1-2H3/t3-,4+
InChI key
BXXWFOGWXLJPPA-ZXZARUISSA-N
General description
meso-2,3-Dibromobutane is a dihaloalkane. It has two forms of rotational isomers, the trans and gauche isomer.[1] The synthesis and dehalogenation reaction of meso-2,3-dibromobutane has been reported.[2] Its IR and Raman spectra have been investigated.[3] The NMR study of the different conformations of meso-2,3-dibromobutane have been reported.[4]
Application
meso-2,3-Dibromobutane is suitable for use in the synthesis of haloalcohol catalyzed by haloalkane dehalogenases.[5]
signalword
Warning
hcodes
pcodes
Hazard Classifications
Eye Irrit. 2
Storage Class
10 - Combustible liquids
wgk_germany
WGK 3
flash_point_f
221.0 °F - closed cup
flash_point_c
105 °C - closed cup
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
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Medium effects in rotational isomerism. VI. Inclusion of dipole-dipole interactions in polar solvents.
Abraham RJ.
The Journal of Physical Chemistry, 73(5), 1192-1199 (1969)
Haloalkane dehalogenase catalysed desymmetrisation and tandem kinetic resolution for the preparation of chiral haloalcohols.
Westerbeek A, et al.
Tetrahedron, 68(37), 7645-7650 (2012)
Dehalogenations of 2, 3-dihalobutanes by alkali naphthalenes. CIDNP [chemically induced dynamic nuclear polarization] and stereochemical study.
Garst JF, et al.
Journal of the American Chemical Society, 97(18), 5242-5249 (1975)
Nuclear magnetic resonance study of rotational isomerism in meso-2, 3-dibromobutane.
Deb KK.
The Journal of Physical Chemistry, 71(9), 3095-3098 (1967)
Infrared and Raman studies on meso-and (?)-2, 3-dichloro-and-2, 3-dibromo-butanes.
Park PJD and Wyn-Jones E.
J. Chem. Soc. Sect. A, 4222-4426 (1969)
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